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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2276621Erstellt: 23. Oktober 2026

Bromobenzene → 1-Pentadecyl-3-phenoxybenzene

https://huagongshe.com/de/reaction/2276621

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBromobenzeneHCID 7961—
EduktDimethylacetamideHCID 31374—
EduktHydrogenated cardanolHCID 68146—
EduktPotassiumHCID 5462222—
LösungsmittelWaterHCID 962—
Produkt1-Pentadecyl-3-phenoxybenzeneHCID 17747909—

Reaktionsbedingungen

Temperatur150 °C

Reaktionsschritte

Into the round bottom flask containing potassium salt of 3-pentadecyl phenol is added bromobenzene followed by Cu powder and in a solvent, DMAc (dimethyl acetamide). The reaction mixture is heated at 150° C. for 6 h. After completion of the reaction, the obtained dark colored reaction mixture is poured into water and the Cu salts are removed by filtration. The filtrate is extracted in a solvent, washed with water and dried, purified to obtain arylated product, 1-pentadecyl-3-phenoxybenzene.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09133089B2
Quelldatensatzuspto-grants-2015_09
ORD IDord-098d7520d0d44e888b6a85333b30fb9f
Quellennotizuspto-grants-2015_09