HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalate → 6-Acetyl-3-(2-(4-(6-chlorobenzothiazol-2-yl)piperazin-1-yl)ethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalate | HCID 71081 | — |
| Edukt | 6-Chloro-2-(piperazin-1-yl)-1,3-benzothiazole | HCID 2746595 | — |
| Edukt | HCID 21471856 | HCID 21471856 | — |
| Produkt | 6-Acetyl-3-(2-(4-(6-chlorobenzothiazol-2-yl)piperazin-1-yl)ethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine | HCID 21471999 | 10,9% |
Reaktionsschritte
The reaction and procedure were conducted in a similar manner as in Example 24 using 0.2 g of 6-acetyl-3-(2-chloroethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine and 0.2 g of 1-(6-chlorobenzothiazol-2-yl)piperazine to give 0.04 g of 6-acetyl-3-(2-(4-(6-chlorobenzothiazol-2-yl)piperazin-1-yl)ethyl)-4,5,6,7-tetrahydro-2-methylthieno[2,3-c]pyridine as an oil, m.p. 180° C. (decomposition) as an oxalate thereof.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05691330 |
| Quelldatensatz | uspto-grants-1997_11 |
| ORD ID | ord-0b5093efc8e545ea90787db95e779a3b |
| Quellennotiz | uspto-grants-1997_11 |