HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4,5-Trimethoxybenzonitrile → 3,4,5-Trimethoxybenzylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4,5-Trimethoxybenzonitrile | HCID 15892 | — |
| Edukt | Sodium borohydride | HCID 4311764 | — |
| Katalysator | Cobalt(II) chloride | HCID 24288 | — |
| Produkt | 3,4,5-Trimethoxybenzylamine | HCID 87736 | — |
Reaktionsschritte
The starting material 3,4,5-trimethoxybenzylamine was prepared by reduction of 3,4,5-trimethoxybenzonitrile with cobalt chloride and sodium borohydride, according to the general method described by L. S. Heinzman in J. Am. Chem. Soc., 104, p. 6801 (1980).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05593993 |
| Quelldatensatz | uspto-grants-1997_01 |
| ORD ID | ord-639de94f192645399ff7872f3e99f776 |
| Quellennotiz | uspto-grants-1997_01 |