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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 234071Erstellt: 24. Oktober 2026

1,3-Bis(4-methylphenyl)prop-2-en-1-one → 1-Methyl-4-[3-(4-methylphenyl)propyl]benzene

https://huagongshe.com/de/reaction/234071

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,3-Bis(4-methylphenyl)prop-2-en-1-oneHCID 256552—
KatalysatorPalladiumHCID 23938—
LösungsmittelAcetic AcidHCID 176—
Produkt1-Methyl-4-[3-(4-methylphenyl)propyl]benzeneHCID 57172699,4%

Reaktionsschritte

To a suspension of 2.14 g of 4,4'-dimethylchalcone in 40 ml of acetic acid was added 0.2 g of 5% palladium on carbon. The reaction vessel was purged with hydrogen gas, and the mixture was vigorously stirred at room temperature for 8.5 hours. The reaction mixture was filtered through Celite, and the filtrate was concentrated to give 2.02 g of the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05594081
Quelldatensatzuspto-grants-1997_01
ORD IDord-9c59153766d74092b67b123096222700
Quellennotizuspto-grants-1997_01