HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
8-(Benzo[d][1,3]dioxol-5-yl)-1,4-dioxaspiro[4.5]decan-8-ol → 1,4-Dioxaspiro[4.5]dec-7-ene, 8-(1,3-benzodioxol-5-yl)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 8-(Benzo[d][1,3]dioxol-5-yl)-1,4-dioxaspiro[4.5]decan-8-ol | HCID 10912840 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 1,4-Dioxaspiro[4.5]dec-7-ene, 8-(1,3-benzodioxol-5-yl)- | HCID 13855633 | 73% |
Reaktionsschritte
A solution of 8-(1,3-benzodioxol-5-yl)-1,4dioxaspiro[4.5]decan-8-ol in toluene was reacted as described in example 2 to give the product (73%, mp: 75°-76° C.). Calc'd for C15H16O4 : C, 69.22%; H, 6.20%. Found: C, 69.19%; H, 6.14%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05595993 |
| Quelldatensatz | uspto-grants-1997_01 |
| ORD ID | ord-3f44056f5e04453bb23db5386ccdd54a |
| Quellennotiz | uspto-grants-1997_01 |