HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Ethenylbenzenesulfonamide → N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Ethenylbenzenesulfonamide | HCID 11367403 | — |
| Edukt | 2,4-Dichloro-6-isocyanato-1,3,5-triazine | HCID 13052624 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide | HCID 20218271 | — |
Reaktionsschritte
A solution of 4,6-dichloro-1,3,5-triazin-2-yl isocyanate (0.87 g, 4.5 mmol) in acetonitrile (9 ml) is contacted with 2-ethenylbenzenesulfonamide (0.83 g, 4.5 mmol) and stirred for 16 hours. The mixture is then evaporated under reduced pressure to yield the title compound which is used directly in subsequent reactions.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04640704 |
| Quelldatensatz | uspto-grants-1987_02 |
| ORD ID | ord-1df3afabf3e9489b97b7a1acc5d394dd |
| Quellennotiz | uspto-grants-1987_02 |