HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrazobenzene → 3,5-Pyrazolidinedione, 4-allyl-1,2-diphenyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrazobenzene | HCID 31222 | — |
| Edukt | Diethyl allylmalonate | HCID 74900 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Produkt | 3,5-Pyrazolidinedione, 4-allyl-1,2-diphenyl- | HCID 216684 | 30,2% |
Reaktionsschritte
Prepared from 1,2-diphenylhydrazine (5.2 g; 28.0 mmol), diethyl allylmalonate (5.0 g; 25.0 mmol), and sodium (0.58 g; 25.0 mmol) using the procedure of Example 3. The crude product was recrystallized from absolute ethanol to give 2.21 g (30%) tan crystals, mp 135-137° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06852749B1 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-88925ccce3964f909e9832860eb5636f |
| Quellennotiz | uspto-grants-2005_02 |