HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Iodine → N-methyl-N-p-chlorobenzyl-m-fluoroaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Iodine | HCID 807 | — |
| Edukt | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Edukt | Sodium Acetate | HCID 517045 | — |
| Edukt | 3-fluoro-N-methylaniline | HCID 2759011 | — |
| Produkt | N-methyl-N-p-chlorobenzyl-m-fluoroaniline | HCID 14008649 | — |
Reaktionsschritte
N-methyl-N-p-chlorobenzyl-m-fluoroaniline was prepared from 17.5 grams (0.14 mole) of N-methyl-m-fluoroaniline, 23.7 grams (0.14 mole) p-chlorobenzyl chloride (Aldrich), 11.9 grams anhydrous sodium acetate and 0.12 grams iodine according to the procedure as described in Example III. Yield 25.8 grams (74 percent), boiling point 162°-170° C. at 0.13 mmHg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04644082 |
| Quelldatensatz | uspto-grants-1987_02 |
| ORD ID | ord-ec17b135791349aa87589d5aa58776f1 |
| Quellennotiz | uspto-grants-1987_02 |