HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cinnamyl bromide → 4-[3-((E)-cinnamyloxy)-5-fluorophenyl]-4-ethyl-2,2-dimethyl-1,3-dioxolane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cinnamyl bromide | HCID 5357478 | — |
| Edukt | 4-Ethyl-4-(5-fluoro-3-hydroxyphenyl)-2,2-dimethyl-1,3-dioxolane | HCID 19088699 | — |
| Produkt | 4-[3-((E)-cinnamyloxy)-5-fluorophenyl]-4-ethyl-2,2-dimethyl-1,3-dioxolane | HCID 19756609 | 2% |
Reaktionsschritte
Using the procedure described in Example 6, (E)-cinnamyl bromide was reacted with 4-ethyl-4-(5-fluoro-3-hydroxyphenyl)-2,2-dimethyl-1,3-dioxolane to give 4-[3-((E)-cinnamyloxy)-5-fluorophenyl]-4-ethyl-2,2-dimethyl-1,3-dioxolane in 2% yield, as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05098932 |
| Quelldatensatz | uspto-grants-1992_03 |
| ORD ID | ord-f84fd097ddd948408e3211658c764c83 |
| Quellennotiz | uspto-grants-1992_03 |