HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Hydroxybenzonitrile | HCID 11907 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| Produkt | O-2-cyanophenyl dimethylthiocarbamate | HCID 14795403 | 94% |
Reaktionsschritte
If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05101048 |
| Quelldatensatz | uspto-grants-1992_03 |
| ORD ID | ord-62a3c0ac533743b5b3990520ae9c3fb3 |
| Quellennotiz | uspto-grants-1992_03 |