HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-bromo-N,N-dimethylbenzamide → HCID 58521976, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-bromo-N,N-dimethylbenzamide | HCID 3335826 | — |
| Edukt | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| Produkt | HCID 58521976 | HCID 58521976 | — |
Reaktionsschritte
Following the general method as outlined in Intermediate 20, starting from (4-chloro-2-ethynyl-phenoxy)-acetic acid tert-butyl ester (Intermediate 3) and 3-bromo-N,N-dimethylbenzamide (Intermediate 180), the title compound was obtained as a brown sticky solid after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08273769B2 |
| Quelldatensatz | uspto-grants-2012_09 |
| ORD ID | ord-7e477b5d4ae94c7f8f66875eaa2441cd |
| Quellennotiz | uspto-grants-2012_09 |