HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → 8-Cyclopropyl-6-ethynyl-2,2,4,4-tetramethylchroman
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 8-Cyclopropyl-6-trimethylsilanylethynyl-2,2,4,4-tetramethyl chroman | HCID 18719789 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 8-Cyclopropyl-6-ethynyl-2,2,4,4-tetramethylchroman | HCID 22569006 | — |
Reaktionsschritte
Following general procedure E and using 8-cyclopropyl-6-trimethylsilanylethynyl-2,2,4,4-tetramethyl chroman (Intermediate 33, 0.17 g, 0.68 mmol), methanol and potassium carbonate (0.2 g, 1.47 mmol) the title compound was obtained as an oil (0.064 g, 47%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06855512B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-931d8dd58b1e4edd80381b11ce10f3fb |
| Quellennotiz | uspto-grants-2005_02 |