HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-methoxy-N,N,N',N'-tetramethylmethylenediamine → HCID 57041370, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-methoxy-N,N,N',N'-tetramethylmethylenediamine | HCID 70908 | — |
| Edukt | 1-Tritylpiperidin-4-one | HCID 2748414 | — |
| Produkt | HCID 57041370 | HCID 57041370 | 64% |
Reaktionsschritte
1-Triphenylmethyl-4-piperidone (0.239 g, 0.70 mmol) was added to methoxybis(dimethylamino)methane (1.75 ml) and the reaction mixture was stirred at 50° for sixteen hours. Volatiles were then removed in vacuo to provide a yellow solid, which was triturated with ether, and air dried to give the title product as a light yellow solid (0.179 g, 0.45 mmol, 64% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05214051 |
| Quelldatensatz | uspto-grants-1993_05 |
| ORD ID | ord-d3145a449e0943ad99bd738ddbac25bb |
| Quellennotiz | uspto-grants-1993_05 |