Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Dodecanol | HCID 8193 | — |
| Edukt | Ethyl mandelate | HCID 13050 | — |
| Produkt | Lauryl mandelate | HCID 11587803 | 62,3% |
Reaktionsschritte
A mixture of Novozym® 435 (2.21 g), molecular sieves (18.60 g), 1-dodecanol (3.76 g), and ethyl mandelate (3.61 g) in a 150 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.0 g of lauryl mandelate (56% yield) was obtained as a clear viscous liquid. The purity of the product was >95% as assessed by HPLC-DAD.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07863025B2 |
|---|
| Quelldatensatz | uspto-grants-2011_01 |
|---|
| ORD ID | ord-e4f46e96d3414ea6b1ddb8db33c7ce15 |
|---|
| Quellennotiz | uspto-grants-2011_01 |
|---|
