HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(4-Aminobutyl)-N-methyl carbamic acid tert-butyl ester → {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(4-Aminobutyl)-N-methyl carbamic acid tert-butyl ester | HCID 2756377 | — |
| Edukt | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Edukt | 3,5-Dimethylpyridine-2-carbaldehyde | HCID 18731683 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester | HCID 58997083 | — |
Reaktionsschritte
Using General Procedure B: Reaction of (4-Amino-butyl)-methyl-carbamic acid tert-butyl ester and 3,5-dimethyl-pyridine-2-carbaldehyde with NaBH(OAc)3 in CH2Cl2 gave {4-[(3,5-Dimethyl-pyridin-2-ylmethyl)-amino]-butyl}-methyl-carbamic acid tert-butyl ester as a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07863293B2 |
| Quelldatensatz | uspto-grants-2011_01 |
| ORD ID | ord-cc4bc05c439d4badafba0393c2085ef4 |
| Quellennotiz | uspto-grants-2011_01 |