HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane → 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane | HCID 20165716 | — |
| Katalysator | Nickel | HCID 935 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane | HCID 20165755 | — |
Reaktionsschritte
1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane is dissolved in methanol and hydrogenated at 50 psi with Raney nickel T-1 as a catalyst. The reaction mixture is filtered through Celite and evaporated to yield 1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04698231 |
| Quelldatensatz | uspto-grants-1987_10 |
| ORD ID | ord-072cd696dd184a92a527b40d5e77fb5d |
| Quellennotiz | uspto-grants-1987_10 |