HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(4-methoxyphenyl)-N-methylmethanamine → 4-(N-(4-methoxybenzyl)-N-methylamino)-1-(4-nitrophenyl)piperidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(4-methoxyphenyl)-N-methylmethanamine | HCID 485407 | — |
| Edukt | 1-(4-Nitrophenyl)piperidin-4-one | HCID 3842562 | — |
| Produkt | 4-(N-(4-methoxybenzyl)-N-methylamino)-1-(4-nitrophenyl)piperidine | HCID 19784354 | 72,4% |
Reaktionsschritte
3.0 g (13.6 mmol) of 1-(4-nitrophenyl)-4-piperidone and 2.0 g (13.6 mmol) of N-(4-methoxybenzyl)-N-methylamine were reacted in a similar manner to Example 1. 3.5 g of 4-(N-(4-methoxybenzyl)-N-methylamino)-1-(4-nitrophenyl)piperidine were obtained. Melting point 144°-145° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05260318 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-7f9b91675af14320a1c9c71b9336bdf2 |
| Quellennotiz | uspto-grants-1993_11 |