HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Iodoethane → 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Iodoethane | HCID 6340 | — |
| Edukt | 1-Phenyl-3-(3-methyl-4-pyridyl)butane | HCID 19783297 | — |
| Edukt | Lithium diisopropylamine | HCID 45051747 | — |
| Produkt | 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane | HCID 19783320 | 15,6% |
Reaktionsschritte
2.1 g (9.35 mmol) of 1-phenyl-3-(3-methyl-4-pyridyl)butane, 1.46 g (9.35 mmol) of ethyl iodide and 2 equivalent of lithium-diisopropylamine were reacted in the same manner as in Example 1. The reaction product was purified to obtain 0.37 g of the desired compound (yield: 15.6%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05262420 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-050c0500979a4433a4718a4be18e859c |
| Quellennotiz | uspto-grants-1993_11 |