HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Allyl Mercaptan → 4-Allylsulfanylmethyl-2,2-dimethyl-6-thiophen-3-yl-1,2-dihydroquinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Allyl Mercaptan | HCID 13367 | — |
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | 2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline | HCID 22566532 | — |
| Produkt | 4-Allylsulfanylmethyl-2,2-dimethyl-6-thiophen-3-yl-1,2-dihydroquinoline | HCID 22566534 | — |
Reaktionsschritte
2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline was brominated with NBS using the procedure described in Example 1 and then coupled with allyl mercaptan using the procedure described in Example 2 to provide 22 mg of the title compound as a oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06858627B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-2ae737324b1e4979a5f2376838cc0e72 |
| Quellennotiz | uspto-grants-2005_02 |