HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Phenylethanethiol → 6-(2,5-Dimethoxyphenyl)-2,2-dimethyl-4-phenethylsulfanylmethyl-1,2-dihydroquinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Phenylethanethiol | HCID 78126 | — |
| Edukt | 2,5-Dimethoxyphenylboronic acid | HCID 2734342 | — |
| Edukt | Trifluoromethanesulfonic acid 2,2,4-trimethyl-1,2-dihydroquinolin-6-yl ester | HCID 20760320 | — |
| Produkt | 6-(2,5-Dimethoxyphenyl)-2,2-dimethyl-4-phenethylsulfanylmethyl-1,2-dihydroquinoline | HCID 10343495 | — |
Reaktionsschritte
Trifluoromethanesulfonic acid 2,2,4-trimethyl-1,2-dihydroquinolin-6-yl ester was coupled with 2,5-dimethoxyphenylboronic acid. Bromination and coupling reaction with 2-phenylethanethiol gave 43 mg of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06858627B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-c246b091f79b4c109a44240105e7ca29 |
| Quellennotiz | uspto-grants-2005_02 |