HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyldithiocarbamic acid, dimethylamine → 3,4-Dimethoxy-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Edukt | 3,4-Dimethoxy-beta-nitrostyrene | HCID 222093 | — |
| Lösungsmittel | Carbon Disulfide | HCID 6348 | — |
| Produkt | 3,4-Dimethoxy-alpha-(nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324596 | — |
Reaktionsschritte
As in Example 17, reaction of 3,4-dimethoxy-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 3,4-dimethoxy-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 108° - 110° C. after recrystallization without heating from acetone-methanol solution.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04038288 |
| Quelldatensatz | uspto-grants-1977_07 |
| ORD ID | ord-102d64bcdad54a068c0089d8601f147b |
| Quellennotiz | uspto-grants-1977_07 |