HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pyridine → Cotinine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pyridine | HCID 1049 | — |
| Edukt | Succinic anhydride | HCID 7922 | — |
| Edukt | 3'-Hydroxycotinine, trans- | HCID 107963 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Cotinine | HCID 854019 | — |
Reaktionsschritte
Cotinine hemisuccinate was prepared by dissolving 19 mg of trans-3'-hydroxycotinine in 1 ml of dimethylformamide (Aldrich). 21 mg of succinic anhydride (Aldrich) were added, followed by 15 μl of pyridine (Aldrich). The mixture was incubated overnight at 45° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05527686 |
| Quelldatensatz | uspto-grants-1996_06 |
| ORD ID | ord-7c2cd0ad0eb24c1c8ca3ae468fdcc9cc |
| Quellennotiz | uspto-grants-1996_06 |