HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Beta-Nitrostyrene → alpha-(Nitromethyl)benzyl diethyldithiocarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Beta-Nitrostyrene | HCID 7626 | — |
| Edukt | Diethylammonium diethylcarbamodithioate | HCID 2735004 | — |
| Lösungsmittel | Carbon Disulfide | HCID 6348 | — |
| Produkt | alpha-(Nitromethyl)benzyl diethyldithiocarbamate | HCID 21324593 | — |
Reaktionsschritte
As in Example 17, reaction of β-nitrostyrene with diethylammonium diethyldithiocarbamate in the presence of carbon disulfide gave α-(nitromethyl)benzyl diethyldithiocarbamate melting at 81° C.-82.5° C. when recrystallized without heating from acetone-2-propanol solution.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04148795 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-021db1f139f940299dd9a715ed39cc5e |
| Quellennotiz | uspto-grants-1979_04 |