HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyldithiocarbamic acid, dimethylamine → 3,4-(Methylenedioxy)-alpha-(nitromethyl)benzyl dimethyldithiocarbamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyldithiocarbamic acid, dimethylamine | HCID 11728 | — |
| Edukt | 5-(2-Nitroethenyl)-1,3-benzodioxole | HCID 94945 | — |
| Lösungsmittel | Carbon Disulfide | HCID 6348 | — |
| Produkt | 3,4-(Methylenedioxy)-alpha-(nitromethyl)benzyl dimethyldithiocarbamate | HCID 21324627 | — |
Reaktionsschritte
As in Example 17, reaction of 3,4-(methylenedioxy)-β-nitrostyrene with dimethylammonium dimethyldithiocarbamate in the presence of carbon disulfide gave 3,4-(methylenedioxy)-α-(nitromethyl)benzyl dimethyldithiocarbamate melting at 122° C.-124° C. when recrystallized without heating from acetone-ethanol solution.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04148795 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-c2556666c56a4f38a98f08ccb528d279 |
| Quellennotiz | uspto-grants-1979_04 |