HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Nitrophenol → 1-(Cyclopentyloxy)-2-nitrobenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Nitrophenol | HCID 6947 | — |
| Edukt | Bromocyclopentane | HCID 8728 | — |
| Produkt | 1-(Cyclopentyloxy)-2-nitrobenzene | HCID 22164473 | — |
Reaktionsschritte
In a similar manner as in Example 1, bromocyclopentane was reacted with o-nitrophenol to yield 2-cyclopentoxynitrobenzene; which was reduced to the corresponding aniline; then reacted with N-methylol-5-methylpyrrolidone to form the corresponding N-5-methyl-N-methylenepyrrolidonyl derivative; which was acylated with chloroacetyl chloride to form the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04153446 |
| Quelldatensatz | uspto-grants-1979_05 |
| ORD ID | ord-59c6a960f43e4430b964afb2e83311fb |
| Quellennotiz | uspto-grants-1979_05 |