HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → 1-(8-Bromooctyl)-4,5-diphenyltriazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 1,8-Dibromooctane | HCID 78310 | — |
| Edukt | HCID 178420171 | HCID 178420171 | — |
| Lösungsmittel | Methyl Ethyl Ketone | HCID 6569 | — |
| Produkt | 1-(8-Bromooctyl)-4,5-diphenyltriazole | HCID 22916394 | — |
Reaktionsschritte
4,5-Diphenyl-1,2,3-triazole was treated with 1,8-dibromooctane and potassium carbonate in butanone to give after chromatographic work up the title compound, m.p. 90°-91° C., Found: C, 64.0; H, 6.5; N, 10.1; Br, 19.8%; C22H26BrN3 requires: C, 64.1;H, 6.4; N, 10.2; Br, 19.4%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05648373 |
| Quelldatensatz | uspto-grants-1997_07 |
| ORD ID | ord-12c89d6856e24cfdbb6d901fe40e713f |
| Quellennotiz | uspto-grants-1997_07 |