HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenyl formate → 3-(2'-Methyl-2'-formylaminobutyl)-indole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenyl formate | HCID 74626 | — |
| Edukt | 3-(2'-Amino-2'-methylbutyl)-indole | HCID 21552235 | — |
| Produkt | 3-(2'-Methyl-2'-formylaminobutyl)-indole | HCID 21552229 | — |
Reaktionsschritte
The 3-(2'-methyl-2'-aminobutyl)-indole obtained as reduction product in accordance with Example 1 or 3 was reacted with phenyl formate to yield 3-(2'-methyl-2'-formylaminobutyl)-indole; melting point 121.5°-124.5°C. (from ether). Reduction thereof with LiAlH4 yielded 3-(2'-methyl-2'-methylaminobutyl)-indole having a melting point of 100°-103°C. (from cyclohexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03947584 |
| Quelldatensatz | uspto-grants-1976_03 |
| ORD ID | ord-8f956a4918304bc2a1e7c1de3a525c8b |
| Quellennotiz | uspto-grants-1976_03 |