HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Pyridinamine, 5-bromo-6-methyl- → HCID 86608069, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Pyridinamine, 5-bromo-6-methyl- | HCID 170678 | — |
| Edukt | 3-Ethynyl-7-trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine | HCID 71539732 | — |
| Produkt | HCID 86608069 | HCID 86608069 | — |
Reaktionsschritte
The title compound was prepared from 3-ethynyl-7-trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine (example C.1) (355 mg, 1.0 mmol) and commercially available 6-amino-3-bromo-2-methylpyridine (168 mg, 1.0 mmol) according to general procedure II. Obtained as a dark-red solid (90 mg, 19%). MS (ISP) 462.2 [(M+H)+]; mp 251-254° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07446113B2 |
| Quelldatensatz | uspto-grants-2008_11 |
| ORD ID | ord-fd1830a865714a9c91e0fd1a665bc9cd |
| Quellennotiz | uspto-grants-2008_11 |