HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenethylamine → N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenethylamine | HCID 1001 | — |
| Edukt | 2-(2-Morpholinoethoxy)benzaldehyde | HCID 976593 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine | HCID 21322775 | 85,6% |
Reaktionsschritte
2-[2-(4-Morpholinyl)ethoxy]benzaldehyde (55.9 g) is reacted with 29 g of phenethylamine in 240 ml of toluene following the procedure described in Example 1A to yield 68.8 g of product as an oil, boiling point 204°-210° C. at 0.1-0.2 mm of Hg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04151354 |
| Quelldatensatz | uspto-grants-1979_04 |
| ORD ID | ord-4ac30af58cde4ba28f2ed7a5aea79b00 |
| Quellennotiz | uspto-grants-1979_04 |