HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → 1-Ethenyl-2-(iodomethyl)benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Sodium Iodide | HCID 5238 | — |
| Edukt | 1-(Chloromethyl)-2-ethenylbenzene | HCID 89757 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 1-Ethenyl-2-(iodomethyl)benzene | HCID 15830574 | 95% |
Reaktionsschritte
Dissolve 1-chloromethyl-2-vinyl-benzene (4.0 g, 26 mmol) in acetone (100 mL) and add sodium iodide (4.5 g, 30 mmol). Heat at gentle reflux for 30 minutes. Cool, add water (150 mL) and extract with pentane (200 mL). Dry (MgSO4) and evaporate the solvent in vacuo to give the title compound (95%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05731306 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-e62ed52d8b364ce5b8047d942697fb19 |
| Quellennotiz | uspto-grants-1998_03 |