HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Acetylimidazolidinone → 3-(2-imidazolin-2-ylamino)-2,3,4,5-tetrahydro-1H-3-benzazepin
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Acetylimidazolidinone | HCID 79350 | — |
| Edukt | 3-amino-2,3,4,5-tetrahydro-1H-3-benzazepin | HCID 12931570 | — |
| Produkt | 3-(2-imidazolin-2-ylamino)-2,3,4,5-tetrahydro-1H-3-benzazepin | HCID 23342921 | — |
Reaktionsschritte
5 g of (0.03 M) 3-amino-2,3,4,5-tetrahydro-1H-3-benzazepin and 4.3 g of (0.034 M) 1-acetyl-imidazolidin-2-one are stirred in 50 ml POCL3 for 1 hour at 100° C. The remaining process steps are analogous to those set forth in Example 5.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04221798 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-ca09b85885634a7d906c54626f6893d9 |
| Quellennotiz | uspto-grants-1980_09 |