HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium hydride → HCID 15239119, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Edukt | HCID 15239125 | HCID 15239125 | — |
| Edukt | HCID 178527880 | HCID 178527880 | — |
| Produkt | HCID 15239119 | HCID 15239119 | — |
Reaktionsschritte
Generally following the procedure of Example 7, 2-mercapto-2-thiazoline (0.67 g, 5.6 mmol) is treated with sodium hydride (0.35 g, 7.3 mmol), with cooling, and the resulting sodium salt is reacted with 1-methyl-2-[4-(1methylpropylthio)phenoxy]ethyl bromide (1.70 g, 5.6 mmol) at RT to give 2-{1-methyl-2-[4-(1-methylpropylthio)phenoxy]ethylthio}-2-thiazoline.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05389651 |
| Quelldatensatz | uspto-grants-1995_02 |
| ORD ID | ord-e8df4daf53eb4aa58097930efe075e3b |
| Quellennotiz | uspto-grants-1995_02 |