HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,2-Dichloro-4-isothiocyanatobenzene → 2-(3,4-Dichlorophenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,2-Dichloro-4-isothiocyanatobenzene | HCID 23065 | — |
| Edukt | N-cyclopentylmethyl-N-(2-chloroethyl)ammonium chloride | HCID 18316280 | — |
| Produkt | 2-(3,4-Dichlorophenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine | HCID 18316297 | — |
Reaktionsschritte
2-Hydroxyethylamine was reacted with cyclopentylmethyl bromide according to Method B2a to give N-cyclopentylmethyl-N-(2-hydroxyethyl)amine. The alcohol was reacted with SOCl2 according to Method B7c to give N-cyclopentylmethyl-N-(2-chloroethyl)ammonium chloride. The chloroethylamine was reacted with 3,4-dichlorophenyl isothiocyanate to give 2-(3,4-dichlorophenylimino)-3-(cyclopentylmethyl)-1,3-thiazolidine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06353006B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-7d4e12a7032a427aa23651c4440c29e5 |
| Quellennotiz | uspto-grants-2002_03 |