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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 27885Erstellt: 24. Oktober 2026

Benzoyl fluoride, 4-(trifluoromethoxy)- → 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE

https://huagongshe.com/de/reaction/27885

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzoyl fluoride, 4-(trifluoromethoxy)-HCID 67612—
Edukt1,8-DiaminonaphthaleneHCID 68067—
LösungsmittelTolueneHCID 1140—
Produkt2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDEHCID 12945439—

Reaktionsschritte

1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04224326
Quelldatensatzuspto-grants-1980_09
ORD IDord-ef9f817d260c40a48ed57129ebeb83cc
Quellennotizuspto-grants-1980_09