HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoyl fluoride, 4-(trifluoromethoxy)- → 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoyl fluoride, 4-(trifluoromethoxy)- | HCID 67612 | — |
| Edukt | 1,8-Diaminonaphthalene | HCID 68067 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE | HCID 12945439 | — |
Reaktionsschritte
1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04224326 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-ef9f817d260c40a48ed57129ebeb83cc |
| Quellennotiz | uspto-grants-1980_09 |