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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 28093Erstellt: 24. Oktober 2026

Lithium Chloride → Benzonitrile, 2,3,6-trichloro-

https://huagongshe.com/de/reaction/28093

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktLithium ChlorideHCID 433294—
Edukt2,3-Dichloro-6-nitrobenzonitrileHCID 2736020—
EduktAluminum(III) ChlorideHCID 6451240—
LösungsmittelN-methyl-2-pyrrolidoneHCID 13387—
ProduktBenzonitrile, 2,3,6-trichloro-HCID 301430791,9%

Reaktionsschritte

10.9 parts of 2,3-dichloro-6-nitrobenzonitrile, 0.84 parts of lithium chloride, 2.22 parts of anhydrous aluminum chloride and 15 parts of N-methyl-2-pyrrolidone were reacted at 180° C. for one hour, and the reaction solution was treated similarly to EXAMPLE B12 to obtain 9.4 parts of 2,3,6-trichlorobenzonitrile with purity of almost 100%. Yield: 91.9%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04225534
Quelldatensatzuspto-grants-1980_09
ORD IDord-559ca7f36b6e4ec28ab2984c9dcfbf89
Quellennotizuspto-grants-1980_09