HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(2,2-Diethyl-1,3-dioxan-5-yl)methanol → 2-(((4-((2,2-Diethyl-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (2,2-Diethyl-1,3-dioxan-5-yl)methanol | HCID 14629254 | — |
| Edukt | 2-(((4-((2-Methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776002 | — |
| Produkt | 2-(((4-((2,2-Diethyl-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776679 | 9,7% |
Reaktionsschritte
The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using (2,2-diethyl-1,3-dioxan-5-yl)methanol obtained in the step (23a) to obtain the title compound (164 mg, total yield: 9.7%) as a light yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07425634B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-81a9d7e6c383445ba117fb9ce0154a93 |
| Quellennotiz | uspto-grants-2008_09 |