HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(Benzyloxy)benzaldehyde → HCID 22009001, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(Benzyloxy)benzaldehyde | HCID 344784 | — |
| Edukt | HCID 178418507 | HCID 178418507 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 22009001 | HCID 22009001 | — |
Reaktionsschritte
2-(benzyloxy)benzaldehyde (5g, 23.6 mmol) was reacted with vinylmagnesium bromide in THF (90 ml) at 0 C. The reaction was quenched with 2 N HCl and the product was extracted in i-PrOAc, dried over Na2SO4 and purified by flash chromatography with EtOAc:toluene 2.5:97.5.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06211197B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-a4708b1709d247f8a0d9098dd75df039 |
| Quellennotiz | uspto-grants-2001_04 |