HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Dichloroacetone → HCID 22009628, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Dichloroacetone | HCID 10793 | — |
| Edukt | 3,5-Dimethylbenzamide | HCID 319485 | — |
| Produkt | HCID 22009628 | HCID 22009628 | 52% |
Reaktionsschritte
In substantially the same manner as in Reference Example 31, 3,5-dimethylbenzamide was allowed to react with 1,3-dichloroacetone to give 4-chloromethyl-2-(3,5-dimethylphenyl)oxazole. The yield was 52%. Recrystallization from isopropyl ether gave colorless needles, mp 76-77° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06211215B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-3ab89e7985c0403891800f8cfb004588 |
| Quellennotiz | uspto-grants-2001_04 |