HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-[3-(3-Hydroxyphenyl)propyl]imidazole → HCID 22009625, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-[3-(3-Hydroxyphenyl)propyl]imidazole | HCID 22009809 | — |
| Edukt | 2-(4-Benzyloxy-phenyl)-4-chloromethyl-oxazole | HCID 22009845 | — |
| Produkt | HCID 22009625 | HCID 22009625 | 81% |
Reaktionsschritte
In substantially the same manner as in Working Example 72, 1-[3-(3-(3-hydroxyphenyl)propyl]imidazole was allowed to react with 2-(4-benzyloxyphenyl)-4-chloromethyloxazole to give 2-(4-benzyloxyphenyl)-4-[3-[3-(1-imidazolyl)propyl]phenoxymethyl]oxazole. The yield was 81%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 144-145° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06211215B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-b40a9129cf504fcc8cbcba254d087a33 |
| Quellennotiz | uspto-grants-2001_04 |