HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Cyanobenzaldehyde → [4-(Aminomethyl)phenyl]methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Cyanobenzaldehyde | HCID 66042 | — |
| Edukt | [3,5-Bis(benzyloxy)benzyl]amine hydrochloride | HCID 15505554 | — |
| Produkt | [4-(Aminomethyl)phenyl]methanol | HCID 6496943 | 46% |
Reaktionsschritte
This compound was prepared by reduction of 4-cyanobenzaldehyde according to the procedure described in preparation of 3,5-dibenzyloxybenzylamine. Yield was 46%: MP 102-123° C.; 1H NMR (Acetone-d6, 500 MHz) 7.27 (m, complex 4H), 4.58 (s, 2H), 3.72 (s, 2H), 3.69 (s, 1H) 2.77 (br, 1H), 2.45 (br, 1H);
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07427608B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-b108a33eb56d42ed8a2fc4baf57a0a48 |
| Quellennotiz | uspto-grants-2008_09 |