HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzylamine → N-Benzyl-2-chloro-9-isopropyl-9H-purin-6-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzylamine | HCID 7504 | — |
| Edukt | 2,6-dichloro-9-(propan-2-yl)-9H-purine | HCID 11218490 | — |
| Lösungsmittel | 1-Butanol | HCID 263 | — |
| Produkt | N-Benzyl-2-chloro-9-isopropyl-9H-purin-6-amine | HCID 10733091 | 85% |
Reaktionsschritte
2,6-dichloro-9-isopropylpurine (1 mmol) and benzylamine (3,5 mmol) were heated with stirring in 3 ml of n-butanol (3 hour, 110° C.). The reaction mixture (after evaporation of n-butanol) was worked up as above for the compound 2, yield 85-90%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06221873B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-ac9cf80d86554577856267a8dbe0d929 |
| Quellennotiz | uspto-grants-2001_04 |