HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Calcium Chloride → HCID 21439120, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Calcium Chloride | HCID 5284359 | — |
| Edukt | sodium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate | HCID 23670418 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 21439120 | HCID 21439120 | — |
Reaktionsschritte
25.2 G. of sodium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate in 300 ml. of water is added to a mixture of 5.55 g. of calcium chloride in 300 ml. of water, and the mixture is allowed to stand for 12 hrs. at room temperature. The mixture is then filtered, and the filtered salt washed several times with portions of ice cold water. The washed salt is dried under vacuum to yield calcium 2-(5-oxo-5H-dibenzo[a,d]cyclohepten-2-yl)propionate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04020094 |
| Quelldatensatz | uspto-grants-1977_04 |
| ORD ID | ord-5b5b2fc142994dc49ee144bd0c4aa90e |
| Quellennotiz | uspto-grants-1977_04 |