HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenol → Phenyl 3-(o-tolyl)propanoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenol | HCID 996 | — |
| Edukt | 3-(2-Methylphenyl)propanoyl chloride | HCID 13029201 | — |
| Produkt | Phenyl 3-(o-tolyl)propanoate | HCID 86715420 | 93% |
Reaktionsschritte
The procedure as described in Example 4a) was repeated with phenol (48 mmol) and 3-o-tolylpropanoyl chloride (55 mmol). The crude product (12.4 g, 97%) was short path distilled at 127-129° C./0.05 mbar to yield 10.6 g (93%) of product as a colourless, semicrystalline oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08877704B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-653a29921ad541cd957e9893431a59c5 |
| Quellennotiz | uspto-grants-2014_11 |