Water → 4-(4-Nitrophenyl)morpholine

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A mixture of 24.5 g morpholine and 13.3 g 1-Fluoro-4-nitro-benzene in 30 ml DMSO was heated to 100° C. for 4 h. This solution was poured on to 300 ml of water and the resulting precipitate was collected by filtration to yield a bright yellow crystalline product, which was dried in vacuo.

Herkunft & Nachweise