HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Phenylbenzaldehyde → HCID 71678680, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Phenylbenzaldehyde | HCID 121053 | — |
| Edukt | 1-(3,4-Dimethoxyphenyl)piperazine | HCID 2736207 | — |
| Edukt | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Edukt | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Produkt | HCID 71678680 | HCID 71678680 | — |
Reaktionsschritte
166.8 mg of the target compound (0.43 mmol, 78.0%) was obtained using 1-(3,4-dimethoxyphenyl)piperazine (244.5 mg, 1.10 mmol), biphenyl-3-carbaldehyde (100 mg, 0.55 mmol) and NaBH(OAc)3 (355 mg, 1.65 mmol) according to the synthesis method of Compound 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08883796B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-3d7348e785894027acab539b691831e1 |
| Quellennotiz | uspto-grants-2014_11 |