HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Allyl bromide → 2-Propenyloxydibenzofuran
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Allyl bromide | HCID 7841 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 2-Dibenzofuranol | HCID 66587 | — |
| Produkt | 2-Propenyloxydibenzofuran | HCID 57252405 | — |
Reaktionsschritte
A solution of 2-hydroxydibenzofuran (2.0 grams) was treated with allyl bromide (1.2 mL) and potassium carbonate (1.5 grams). The mixture was stirred over night at 60°. The reaction was partitioned between methylene chloride and water. The organic was washed once with water and dried over sodium sulfate. The organic layer was filtered and concentrated to an oil which was chromatographed over silica gel to afford the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05859051 |
| Quelldatensatz | uspto-grants-1999_01 |
| ORD ID | ord-3e18335d1be24ab18925c6d52005670c |
| Quellennotiz | uspto-grants-1999_01 |