HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzaldehyde → Ethyl 2-benzylideneaminobutyrate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzaldehyde | HCID 240 | — |
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | Ethyl 2-Aminobutyrate Hydrochloride | HCID 12844023 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | Ethyl 2-benzylideneaminobutyrate | HCID 10331026 | — |
Reaktionsschritte
Triethylamine (2 moles) was added to a solution of the product from step (a) (1 mole) in toluene. When addition was complete, benzaldehyde (1 mole) was added. The mixture was azeotroped until no further water was collected, then cooled to room temperature and filtered. The filtrate was evaporated in vacuo ti give the desired product as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05859240 |
| Quelldatensatz | uspto-grants-1999_01 |
| ORD ID | ord-410984a921a147c6bb9ce5296f537673 |
| Quellennotiz | uspto-grants-1999_01 |