HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → 2-Benzylcyclohexan-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Benzyl Chloride | HCID 7503 | — |
| Edukt | Pyrrolidine, 1-cyclohexyl- | HCID 139064 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | 2-Benzylcyclohexan-1-one | HCID 98945 | — |
Reaktionsschritte
A mixture of 1-(1-pyrrolidinyl)cyclohexane (85.4 g) and benzyl chloride (100 ml) in dioxane (400 ml) was heated under reflux for 23 hours under nitrogen. Water (100 ml) was then added and the brown oil was distilled to give (2RS)-2-phenylmethylcyclohexanone (47.1 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05057513 |
| Quelldatensatz | uspto-grants-1991_10 |
| ORD ID | ord-21da1710588a4bcabd47799acedec4b2 |
| Quellennotiz | uspto-grants-1991_10 |