HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Imidazole → HCID 23511477, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Imidazole | HCID 795 | — |
| Edukt | tert-Butyldimethylsilane | HCID 5072427 | — |
| Edukt | 4-(Hydroxymethyl)-5-methyl-1,3-dioxol-2-one | HCID 10510878 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | HCID 23511477 | HCID 23511477 | — |
Reaktionsschritte
A solution of 5-methyl-4-hydroxymethyl-2-oxo-1,3-dioxolene (1 mmole) in DMF was treated with tert-butyldimethylsilane (1.2 mmole) and imidazole (2.2 mmole) at 25° C. for 24 h. Extraction and chromatography gave 5-methyl-4-tert-butyldimethylsilyloxymethyl-2-oxo-1,3-dioxolene.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06756360B1 |
| Quelldatensatz | uspto-grants-2004_06 |
| ORD ID | ord-e740a62547524ca48f9b5d1ddf9d1883 |
| Quellennotiz | uspto-grants-2004_06 |