HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium hydride → HCID 12961164, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 5-Nitro-2,3-dihydro-1,3-benzoxazol-2-one | HCID 263965 | — |
| Edukt | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | HCID 12961164 | HCID 12961164 | — |
Reaktionsschritte
The product is produced as described in example 1 from 6 g. of NaH (80% suspension in mineral oil), 36 g. of 5-nitrobenzoxazolin-2-one (produced in usual manner by reacting 2-amino-4-nitrophenol-hydrochloride with phosgene), 400 cc. of DMF, 47.4 g. of 8-bromo caprylic acid methyl ester and 6 g. of NaJ.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04377695 |
| Quelldatensatz | uspto-grants-1983_03 |
| ORD ID | ord-5083d77515734e688cceec493cc3548a |
| Quellennotiz | uspto-grants-1983_03 |